Dichlorination of olefins with NCS/Ph(3)P.

Yasumasa Kamada, Yuta Kitamura, Tetsuaki Tanaka, Takehiko Yoshimitsu

Graduate School of Pharmaceutical Sciences, Osaka University, 1-6 Yamadaoka, Suita, Osaka 565-0871, Japan.

Organic & biomolecular chemistry 2013 Feb 13

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A 2 : 1 mixture of NCS and Ph(3)P successfully promoted the anti-dichlorination of olefins to provide corresponding dichlorides, serving as a molecular chlorine surrogate generated in situ.

Citation

Yasumasa Kamada, Yuta Kitamura, Tetsuaki Tanaka, Takehiko Yoshimitsu. Dichlorination of olefins with NCS/Ph(3)P. Organic & biomolecular chemistry. 2013 Feb 13;11(10):1598-601

PMID: 23364517

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