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A simple synthetic method is presented for the precipitation of high purity, dry amorphous calcium carbonate (ACC) based on freeze-drying saturated, counter ion free CaCO3 solutions, where the ACC produced shows an extended atmospheric stability. Translation of the methodology to amorphous calcium phosphate demonstrates the generality of the approach.


Johannes Ihli, Alexander N Kulak, Fiona C Meldrum. Freeze-drying yields stable and pure amorphous calcium carbonate (ACC). Chemical communications (Cambridge, England). 2013 Apr 18;49(30):3134-6

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PMID: 23478859

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