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A direct transformation of N-aryl formamides to the corresponding carbamates via the formation of isocyanate intermediates is achieved in good yields using hypervalent iodine as an oxidant.

Citation

N Veera Reddy, K Rajendra Prasad, P Sudhir Reddy, M Lakshmi Kantam, K Rajender Reddy. Metal free oxidative coupling of aryl formamides with alcohols for the synthesis of carbamates. Organic & biomolecular chemistry. 2014 Apr 14;12(14):2172-5

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PMID: 24569949

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