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    Phenethyl glycosides having phenolic or methoxy functions at benzene rings are substances widely occurring in nature. This kind of compounds has been shown to have anti-oxidant, anti-inflammatory, and anticancer activities. However, some of them are not naturally abundant, thus the synthesis of such molecules is desirable. In this paper, natural phenethyl glycosides 3 and 4 were first totally synthesized from easily available materials with overall yields of 50.5% and 40.1%, respectively. And a new synthetic route to obtain natural phenethyl glycoside 2 in 46.2% yield was also described.


    Hong-Bo Dong, Jian Meng, Zhong-Quan Yao, Hong-Bing Luo, Jing-Xia Zhang, Wei-Hong Du, Ke-Hui Tang, Sheng-Hua Cao. Total synthesis of three natural phenethyl glycosides. Journal of Asian natural products research. 2021 Mar;23(3):284-293

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    PMID: 32079415

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