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Chemospecific C3- and C2-Olefinations of Isatins by TfOH-Promoted Tandem Aldol-Grob and Semiacetalization-Grob Fragmentations.

Hongchen Li, Lidong Shan, Chulong Liu, Nan Liu, Xinyan Wang, Yuefei Hu

Organic letters 2023 Jun 30


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  • aldehydes (2)
  • amides (3)
  • isatins (5)
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    A novel method for TfOH-promoted chemospecific C3- and C2-olefinations of isatins is developed, which offers the first examples of Grob fragmentation using isatins and amides as substrates.

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    Hongchen Li, Lidong Shan, Chulong Liu, Nan Liu, Xinyan Wang, Yuefei Hu. Chemospecific C3- and C2-Olefinations of Isatins by TfOH-Promoted Tandem Aldol-Grob and Semiacetalization-Grob Fragmentations. Organic letters. 2023 Jun 30;25(25):4656-4660

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    PMID: 37318838

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